What you'll learn
Understand the Principles behind Binary Distillation
Design & Operate Flashing, and Flash Drums via Flash Distillation of Binary Mixtures
Understand and apply the principles and methods for simple distillation of binary mixtures
Understand Continuous Distillation Equipment
Model Distillations of Binary Systems
Apply McCabe-Thiele Method for Continuous Distillation Column Design (Number of Stages)
Simulate several process, specially continuous and batch distillation of binary mixtures
Get to know the "Recycle Ratio", "Reboiler Duty", "Feed Stage" etc...
Model Stripping and Enriching Sections of a Distillation Column
Requirements
Mass Transfer Basics
Transport Phenomena
Thermodynamics
Mass and Energy Balances
Physical Chemistry
Description
Introduction:Binary Distillation is one of the most important Mass Transfer Operations used extensively in the Chemical industry.Understanding the concept behind Gas-Gas, Liquid-Liquid and the Gas-Liquid mass transfer interaction will allow you to understand and model Distillation Columns, Flashes, Batch Distillator, Tray Columns and Packed column, etc...We will cover:REVIEW: Of Mass Transfer Basics (Equilibrium VLE Diagrams, Volatility, Raoult's Law, Azeotropes, etc..)Distillation TheoryApplication of Distillation in the IndustryCounter-Current Operation Several equipment to Carry Gas-Liquid OperationsBubble, Spray, Packed and Tray Column equipmentFlash Distillation & Flash Drums DesignDesign & Operation of Tray ColumnsNumber of Ideal Stages: McCabe Thiele Method & Ponchon Savarit MethodRecycleCondenser types: partial, totalPressure drop due to traysDesign & Operation of Packed Columns Pressure drop due to traysEfficiency of Stages & Murphree's EfficencyBatch Distillation, the Raleigh EquationSoftware Simulation for Absorption/Stripping Operations (ASPEN PLUS/HYSYS)Solved-Problem Approach:All theory is backed with exercises, solved problems, and proposed problems for homework/individual study.At the end of the course:You will be able to understand mass transfer mechanism and processes behind Binary Distillation in Flash, Continuous & Batch Processes. You will be able to continue with a Multi-Component Distillation, Reactive Distillation and Azeotropic Distillation as well as more Mass Transfer Unit Operation Courses and/or Separation Processes Course.About your instructor:I majored in Chemical Engineering with a minor in Industrial Engineering back in 2012.I worked as a Process Design/Operation Engineer in INEOS Koln, mostly on the petrochemical area relating to naphtha treating. There I designed and modeled several processes relating separation of isopentane/pentane mixtures, catalytic reactors and separation processes such as distillation columns, flash separation devices and transportation of tank-trucks of product.
Overview
Section 1: Welcome!
Lecture 1 Introduction to Distillation
Lecture 2 Requirements
Lecture 3 Reference Material
Section 2: Review of Mass Transfer & Transport Phenomena
Lecture 4 Ideal Gas
Lecture 5 Ideal Solution
Lecture 6 Vapor Pressure
Lecture 7 Partial Pressure
Lecture 8 What is Equilibrium? (Pure Substances)
Lecture 9 Raoult's Law
Lecture 10 What is Flux?
Lecture 11 What is Ja? Diffusion Flux
Lecture 12 Convection
Section 3: Binary Distillation Overview
Lecture 13 Type of Equipment - Dispersion of Gas-Liquid and Liquid-Gas
Lecture 14 Spray Column
Lecture 15 Bubble Column
Lecture 16 Packed Column
Lecture 17 Tray Column
Lecture 18 Types of Operation
Lecture 19 Single vs. Multiple Stage
Lecture 20 Introduction to Tray Columns
Lecture 21 Sieve Trays
Lecture 22 Valve Trays
Lecture 23 Bubble Cap Trays
Lecture 24 Tray Considerations
Lecture 25 Trays - Spacing
Lecture 26 Trays - Sizing
Lecture 27 Trays - Layouts
Lecture 28 Trays - Materials
Lecture 29 Trays - Manways
Lecture 30 Trays - Operations
Lecture 31 Tray - Pressure Drop
Lecture 32 Trays - Costs
Lecture 33 Tray - Maintenance
Lecture 34 Trays - Summary
Lecture 35 All other Pieces
Lecture 36 Bubbling Area
Lecture 37 Contact Area
Lecture 38 Weir
Lecture 39 Downcomer
Lecture 40 Stage Efficiency
Lecture 41 Murphree's Efficiency
Lecture 42 Column Operation
Lecture 43 Column Operation - Normal
Lecture 44 Column Operation - Flooding
Lecture 45 Column Operation - Priming
Lecture 46 Column Operation - Coning
Lecture 47 Column Operation - Weeping
Lecture 48 Column Operation - Dumping
Lecture 49 Column Operation - Summary
Lecture 50 Tray Diameter Introduction
Lecture 51 Tray Spacing
Lecture 52 Pressure Drop in Trays
Lecture 53 Hd, Dry Liquid sieve loss - Pressure Drop in trays
Lecture 54 Hl, (equivalent h eight of clear liquid holdup)
Lecture 55 Hd, Surface Tension Pressure loss
Lecture 56 Packed Columns vs. Tray Columns
Lecture 57 Introduction to Packings
Lecture 58 Packing Material
Lecture 59 Random Packing
Lecture 60 Stacked Packing
Lecture 61 Structural Packing
Lecture 62 Other Column Internals
Lecture 63 Liquid distributor
Lecture 64 Liquid/Vapour Re-Distributor
Lecture 65 Vapour Distributor
Lecture 66 Demister / Mist Eliminator
Lecture 67 Vortex breaker
Lecture 68 Packing Supports
Lecture 69 Retaining devices (Hold-down Plate & Bed limiter )
Lecture 70 Column Structure - Top
Lecture 71 Column Structure - Middle
Lecture 72 Column Structure - Bottom
Section 4: Software Simulation
Lecture 73 Benzene and toluene Feed Tray, Min. Recycle Ratio, etc
Lecture 74 WKS RadFrac - C3 - iC4 Separation - Recycle
Lecture 75 WKS RadFrac - Column Internals, Trays vs Packings
Lecture 76 WKS Sensitivity Analysis of Feed Stages, Reflux Ratios and Pressure in a RadFrac
Section 5: Bonus
Lecture 77 Surprise!
Chemical Engineers refreshing their Mass Transfer and Separation Processes course,Students on the relevant fields (chemical, mechanical, process engineering),Engineers working with Distillation Columns / Flash Drums,Process Separation Engineer

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